gravimetric determination of nickel with cyclohexylidine-ammonium-2-aminoc yclohexy lidine- 1-cyclohexene-1-dithiocarboxylate
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abstract
cyclohexylidine-ammonium-2-aminocyclohexyline-l-cyclohexee-l- dithiocarboxylate (cccd) is employed for the gravimetric determination of ni (ii). in neutral or ammoniacal solutions, the metal forms a violet precipitate with the reagent which can be weighed as ni (c13h18ns2)a2f ter drying at 115 - 120?c using this procedure, the nickel content of steel samples can also be determined accurately. the purity of the precipitate and complete removal of interferences are confirmed by differential pulse polarography
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GRAVIMETRIC DETERMINATION OF NICKEL WITH CYCLOHEXYLIDINE-AMMONIUM-2-AMINOC YCLOHEXY LIDINE- 1-CYCLOHEXENE-1-DITHIOCARBOXYLATE
Cyclohexylidine-ammonium-2-aminocyclohexyline-l-cyclohexee-l- dithiocarboxylate (CCCD) is employed for the gravimetric determination of Ni (II). In neutral or ammoniacal solutions, the metal forms a violet precipitate with the reagent which can be weighed as Ni (C13H18NS2)a2f ter drying at 115 - 120?C Using this procedure, the nickel content of steel samples can also be determined accurate...
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Journal title:
journal of sciences islamic republic of iranجلد ۱، شماره ۱، صفحات ۰-۰
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